By Thomas J. Pinnavaia, M. F. Thorpe
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By using an ensemble of organic molecules to create a larger template, this method has been extended to the synthesis of ordered mesoporous materials. 5-10 Four reagents are necessary: a source of the small metal-oxide ions, a surfactant, a solvent, and a chemical to adjust the pH. In our syntheses, we introduce a source of silica (tetramethoxysilane, TMOS) into a basic aqueous solution of a micelle-forming cationic surfactant. The TMOS is hydrolyzed to form small anionic oligomers that can coordinate with the surfactant headgroups.
Sci. , vol. 84, J. G. Karge, H. Pfeifer, and W. , Elsevier, Amsterdam (1994), pp. 69-75. 51. J. T. Tanev, W. Jialiang, and W. Zhang, Ti-substituted mesoporous molecular sieves for catalytic oxidation of large aromatic compounds prepared by neutral templating route, in: “Advances in Porous Materials,” Sh. S. M. , MRS Symp. Proc. , vol. 371, Pittsburgh, (1995), pp. 53-62. 52. S. Reddy, A. Dicko, and A. Sayari, Ti-modified mesoporous molecular sieves, TiMCM-41 and Ti-HMS, in: “ACS Symp. , Proceedings of the Division of Petroleum Chemistry,” Anheim, CA (in press).
L. Moudrakovski, Synthesis, characterization and modification of MCM-41 molecular sieves, in: “Advances in Porous Materials,” Sh. S. M. , MRS Symp. Proc. , vol. 371, Pittsburgh (1995). 48. M. Reddy, I. Moudrakovski, and A. Sayari, Synthesis of mesoporous vanadium silicate molecular sieves, J. Chem. Soc. Chem. Commun. 1994, 1059. 49. B. E. Davis, Catalytic activity of titanium silicates synthesized in the presence of alkali metal and alkaline earth ions, J. Catal. B. B. A. E. Davis, Studies on the catalytic oxidation of alkanes and alkenes by titanium silicates, J.
Access in nanoporous materials by Thomas J. Pinnavaia, M. F. Thorpe